2,5-diiodo-4-methylphenethyl alcohol

Base Information

Chemical Name:2,5-diiodo-4-methylphenethyl alcohol
CAS No.:615570-04-2
Molecular Formula:C₉H₁₀I₂O
Molecular Weight:387.987
Hs Code.:

Synonyms:2,5-diiodo-4-methylphenethyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-diiodo-4-methylphenethyl alcohol

Chemical Property:

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Technology Process of 2,5-diiodo-4-methylphenethyl alcohol

There total 3 articles about 2,5-diiodo-4-methylphenethyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2,5-diiodo-4-methylphenethyl acetate

: 615570-04-2
2,5-diiodo-4-methylphenethyl alcohol

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1039/b303699p

Reference yield:

: 699-02-5
4-Methylphenethyl alcohol

: 615570-04-2
2,5-diiodo-4-methylphenethyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 4-dimethylaminopyridine / pyridine / 6 h / 20 °C

2: 78 percent / I₂; H₅IO₆; H₂SO₄ / acetic acid; H₂O / 3 h / 80 °C

3: 93 percent / K₂CO₃ / methanol; CH₂Cl₂ / 16 h / 20 °C

With dmap; sulfuric acid; iodine; potassium carbonate; periodic acid; In pyridine; methanol; dichloromethane; water; acetic acid;
DOI:10.1039/b303699p

Reference yield:

: 22532-47-4
4-methylphenethyl acetate

: 615570-04-2
2,5-diiodo-4-methylphenethyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / I₂; H₅IO₆; H₂SO₄ / acetic acid; H₂O / 3 h / 80 °C

2: 93 percent / K₂CO₃ / methanol; CH₂Cl₂ / 16 h / 20 °C

With sulfuric acid; iodine; potassium carbonate; periodic acid; In methanol; dichloromethane; water; acetic acid;
DOI:10.1039/b303699p