2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

Base Information

Chemical Name:2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose
CAS No.:869213-46-7
Molecular Formula:C₃₃H₄₂O₇Si
Molecular Weight:578.778
Hs Code.:

Synonyms:2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

Suppliers and Price of 2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

There total 2 articles about 2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1391099-66-3
2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranose

: 69739-34-0
t-butyldimethylsiyl triflate

: 869213-46-7
2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo301189y

Reference yield:

: C₂₇H₂₆O₆

: 869213-46-7
2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; hydrogen / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

3: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; boron trifluoride diethyl etherate; hydrogen; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo301189y