2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

Base Information

Chemical Name:2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate
CAS No.:92982-67-7
Molecular Formula:C₂₇H₃₄Br₃O₁₀P
Molecular Weight:789.247
Hs Code.:

Synonyms:2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

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Chemical Property of 2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

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Technology Process of 2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

There total 9 articles about 2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 92982-65-5
2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2-O-benzyl-O-(1-propenyl)-sn-glycer-3-yl 2,2,2-tribromoethyl phosphate

: 92982-67-7
2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetone; at 20 ℃; for 0.75h;
DOI:10.1016/0008-6215(84)85277-5

Reference yield:

: 106401-57-4
1-O-allyl-2-O-benzyl-sn-glycerol

: 92982-67-7
2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / pyridine, 4-dimethylaminopyridine / dioxane / 3 h / 20 °C

2: 97 percent / 1,5-cyclooctadienebisiridinium hexafluorophosphate / various solvent(s) / 2 h / 20 °C

3: 91 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

4: 1.) pyridine, 2.) 1-methylimidazole / 1.) oxolane, 20 deg C, 20 min, 2.) oxolane, 20 deg C, 2.5 h

5: 97 percent / mercuric oxide, mercuric chloride / acetone; H₂O / 0.75 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; dmap; hydrazine hydrate; acetic acid; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; In 1,4-dioxane; water; acetone;
DOI:10.1016/0008-6215(84)85277-5

Reference yield:

: 117606-89-0
1-O-trityl-2-O-benzyl-3-O-allyl-sn-glycerol

: 92982-67-7
2-O-benzyl-sn-glycer-3-yl 2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycer-1-yl 2,2,2-tribromoethyl phosphate

Guidance literature:: Multi-step reaction with 6 steps

1: M hydrogen chloride / methanol; dioxane / 0.33 h

2: 86 percent / pyridine, 4-dimethylaminopyridine / dioxane / 3 h / 20 °C

3: 97 percent / 1,5-cyclooctadienebisiridinium hexafluorophosphate / various solvent(s) / 2 h / 20 °C

4: 91 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

5: 1.) pyridine, 2.) 1-methylimidazole / 1.) oxolane, 20 deg C, 20 min, 2.) oxolane, 20 deg C, 2.5 h

6: 97 percent / mercuric oxide, mercuric chloride / acetone; H₂O / 0.75 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; hydrogenchloride; dmap; hydrazine hydrate; acetic acid; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; In 1,4-dioxane; methanol; water; acetone;
DOI:10.1016/0008-6215(84)85277-5