4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

Base Information

Chemical Name:4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine
CAS No.:149695-30-7
Molecular Formula:C₂₅H₃₂N₆O₆
Molecular Weight:512.566
Hs Code.:

Synonyms:4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

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Chemical Property of 4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

Chemical Property:

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Technology Process of 4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

There total 1 articles about 4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-N-(tert-butylbenzoyl)-2'-O-tetrahydropyranylcytydine

: 149695-30-7
4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

Guidance literature:: With lithium azide; carbon tetrabromide; triphenylphosphine; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1021/ja00065a006

Reference yield:

: 149695-30-7
4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

: 149695-36-3
4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-3'-O-(dimethoxytrityl)-5'-N-((9-fluorenylmethoxy)carbonyl)-5'-amino-5'-deoxycytidine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 40 h / 50 °C

2: Et₃N, Ph₃P / methanol / 1.5 h / Ambient temperature

3: pyridine / 0.5 h / Ambient temperature

With pyridine; triethylamine; triphenylphosphine; In methanol;
DOI:10.1021/ja00065a006

Reference yield:

: 149695-30-7
4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-azido-5'-deoxycytidine

: 149695-38-5
4-N-(tert-butylbenzoyl)-2'-O-(tetrahydropyranyl)-5'-N-((9-fluorenylmethoxy)carbonyl)-5'-amino-5'-deoxycytidine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 40 h / 50 °C

2: Et₃N, Ph₃P / methanol / 1.5 h / Ambient temperature

3: pyridine / 0.5 h / Ambient temperature

4: dichloroacetic acid / CH₂Cl₂ / 0.25 h / Ambient temperature

With pyridine; dichloro-acetic acid; triethylamine; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1021/ja00065a006