1-CHLORO-6-PHENYLHEXANE

Base Information

• Chemical Name: 1-CHLORO-6-PHENYLHEXANE
• CAS No.: 71434-68-9
• Molecular Formula: C₁₂H₁₇Cl
• Molecular Weight: 196.72
• Hs Code.: 2903999090
• Mol file: 71434-68-9.mol

Synonyms:1-Chlorohexylbenzene

Chemical Property of 1-CHLORO-6-PHENYLHEXANE

Chemical Property:

• Vapor Pressure: 0.00548mmHg at 25°C
• Refractive Index: 1.5105
• Boiling Point: 88-91°C 0,4mm
• Flash Point: >110°C
• PSA: 0.00000
• Density: 0.981
• LogP: 4.02830
• Solubility.: Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

98%Min ^*data from raw suppliers

6-Phenylhexylchloride ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-CHLORO-6-PHENYLHEXANE

There total 1 articles about 1-CHLORO-6-PHENYLHEXANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 6,6-dichloro-2-oxabicyclo<3.1.0>hexane (24765-58-0) → 1-chloro-1-phenylhexane (71434-68-9) + (6α,6aβ)-3,5,6,6a-Tetrahydro-6-phenyl-2H-cyclobutapyran (121029-48-9) + (6α,6aα)-3,5,6,6a-Tetrahydro-6-phenyl-2H-cyclobutapyran (121029-47-8)

Guidance literature:

With n-butyllithium; In hexane; Yields of byproduct given; 1.) -25 - -30 deg C, 1.5 h; 2.) to 0 deg C in 30 min;

Reference yield:

1-chloro-1-phenylhexane (71434-68-9) → 1-phenylhexan-1-ol (4471-05-0)

Guidance literature:

In ethanol; at 25 ℃; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.);

DOI:10.1021/jo00367a001

upstream raw materials:

styrene

6,6-dichloro-2-oxabicyclo<3.1.0>hexane

Downstream raw materials:

1-phenylhexan-1-ol

Refernces