4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol

Base Information

• Chemical Name: 4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol
• CAS No.: 176646-50-7
• Molecular Formula: C₁₂H₁₉ClS₂Si
• Molecular Weight: 290.953

Synonyms:4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol

Chemical Property of 4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol

Chemical Property:

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Technology Process of 4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol

There total 1 articles about 4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobutanoyl dimethylphenyl silane (161497-73-0) → 4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol (176646-50-7)

Guidance literature:

With hydrogenchloride; hydrogen sulfide; In diethyl ether; at -30 ℃;

DOI:10.1016/0040-4020(96)00148-2

Reference yield: 100.0%

4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol (176646-50-7) → 2-(dimethylphenylsilyl)-thiacyclo pent-2-ene

Guidance literature:

With sodium hydroxide; In diethyl ether;

DOI:10.1016/0040-4020(96)00148-2

Reference yield: 87.0%

4-chloro-1-dimethylphenylsilyl-1,1-butane dithiol (176646-50-7) → (Z)-4-chloro-1-dimethylphenylsilyl-but-1-enethiol

Guidance literature:

With sodium hydrogencarbonate; In diethyl ether;

DOI:10.1016/0040-4020(96)00148-2

upstream raw materials:

4-chlorobutanoyl dimethylphenyl silane

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