[CoFe₂(CC₆H₄CH₃)(CO)10]

Base Information

Chemical Name:[CoFe₂(CC₆H₄CH₃)(CO)10]
CAS No.:106972-25-2
Molecular Formula:C₁₈H₇CoFe₂O₁₀
Molecular Weight:553.935
Hs Code.:

[CoFe<sub>2</sub>(CC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)(CO)10]

Synonyms:[CoFe₂(CC₆H₄CH₃)(CO)10]

Suppliers and Price of [CoFe₂(CC₆H₄CH₃)(CO)10]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [CoFe₂(CC₆H₄CH₃)(CO)10]

Chemical Property:

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Technology Process of [CoFe₂(CC₆H₄CH₃)(CO)10]

There total 1 articles about [CoFe₂(CC₆H₄CH₃)(CO)10] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 15321-51-4
diiron nonacarbonyl

: {CoW(CC₆H₄CH₃)(CO)8}

: 106972-25-2
[CoFe₂(CC₆H₄CH₃)(CO)10]

Guidance literature:: In diethyl ether; byproducts: Fe3(CO)12, W(CO)6, Fe(CO)5; (O2-free N2); soln. of CoW compd. (3.00 mmol) treated with Fe2(CO)9 (9.00 mmol); mixt. stirred at room temp. for 3 h; resulting soln. evapd. (vac.); chromy. on Kieselgel column (light petroleum): 1. band (green) = some Fe3(CO)12; 2. band (dark brown) evapd. (vac); residue crystd. at -78 °C from light petroleum; elem. anal.;
DOI:10.1039/DT9860001723

Reference yield: 92.0%

: 106972-25-2
[CoFe₂(CC₆H₄CH₃)(CO)10]

: 106972-26-3
CoFe₂(CC₆H₄CH₃)(CO)9(P(C₆H₅)3)

Guidance literature:: With PPh₃; In light petroleum; under oxygen-free nitrogen; mixt. stirred at room temp. for 4 h; solvent removed (vac.); chromy. on Kieselgel column (CH2Cl2/light petroleum 1/4); evapn. (vac.) gave microcrystals; elem. anal.;
DOI:10.1039/DT9860001723

Reference yield: 89.0%

: 106972-25-2
[CoFe₂(CC₆H₄CH₃)(CO)10]

: 2071-20-7
bis-diphenylphosphinomethane

: 106972-27-4
CoFe₂(CC₆H₄CH₃)(CO)8((C₆H₅)2PCH₂P(C₆H₅)2)

Guidance literature:: In light petroleum; (O2-free N2); mixt. of CoFe2 compd. (0.20 mmol) and dppm (0.20 mmol) inlight petroleum stirred at room temp. for 3 h; cooling to ca. -40 °C; supernatant liquid removed with syringe; residue crystd. (Et2O, -78 °C); elem. anal.;
DOI:10.1039/DT9860001723