tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

Base Information

Chemical Name:tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate
CAS No.:854757-90-7
Molecular Formula:C₂₉H₃₂N₂O₄
Molecular Weight:472.584
Hs Code.:

Synonyms:tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

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Chemical Property of tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

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Technology Process of tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

There total 1 articles about tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 338462-91-2
3-carbethoxy-5(R)-<1'-(S)-<(tert-butyloxycarbonyl)amino>-2-phenylethyl>dihydrofuran-2(3H)-one

: 52199-24-3
2-[(4-bromomethyl)phenyl]pyridine

: 854757-90-7
tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

Guidance literature:: 3-carbethoxy-5(R)-<1'-(S)-<(tert-butyloxycarbonyl)amino>-2-phenylethyl>dihydrofuran-2(3H)-one; 2-[(4-bromomethyl)phenyl]pyridine; With sodium ethanolate; In ethanol; at 0 - 25 ℃; for 16h;

With lithium hydroxide; water; In ethanol; at 25 ℃; for 5h;

With citric acid; In ethanol; water; pH=5;

Reference yield:

: 854757-90-7
tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate

: C₂₉H₃₄N₂O₅

Guidance literature:: tert-butyl (1S)-1-{(2R)-5-oxo-4-[4-(2-pyridinyl)benzyl]tetrahydro-2-furanyl}-2-phenylethylcarbamate; With sodium hydroxide; water; In 1,4-dioxane; at 25 ℃; for 0.5h;

With citric acid; In 1,4-dioxane; water; at 0 ℃; pH=5;