N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

Base Information

Chemical Name:N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride
CAS No.:1269408-15-2
Molecular Formula:C₁₃H₁₅N₅O₃*ClH
Molecular Weight:325.755
Hs Code.:

N<sub>1</sub>-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

Synonyms:N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

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Chemical Property of N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

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Technology Process of N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

There total 4 articles about N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1269406-72-5
1,1-dimethylethyl (2-{[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]amino}-2-oxoethyl)carbamate

: 1269408-15-2
N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 17h;

Reference yield:

: 17417-09-3
2-fluoro-5-nitrobenzonitrile

: 1269408-15-2
N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 1 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

3: triethylamine; HATU / dichloromethane / 18.5 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 17 h / 20 °C

With hydrogenchloride; potassium carbonate; triethylamine; HATU; In 1,4-dioxane; dichloromethane; acetonitrile;

Reference yield:

: 1269406-69-0
1,1-dimethylethyl [(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]carbamate

: 1269408-15-2
N₁-[(3S)-1-(2-cyano-4-nitrophenyl)-3-pyrrolidinyl]glycinamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2: triethylamine; HATU / dichloromethane / 18.5 h / 20 °C

3: hydrogenchloride / 1,4-dioxane / 17 h / 20 °C

With hydrogenchloride; triethylamine; HATU; In 1,4-dioxane; dichloromethane;