3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate

Base Information

• Chemical Name: 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate
• CAS No.: 868738-76-5
• Molecular Formula: C₃₈H₇₁BrNO₄P
• Molecular Weight: 716.864
• Mol file: 868738-76-5.mol

Synonyms:3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate

Chemical Property of 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate

There total 4 articles about 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

octadecyl N-(2-bromoethyl)-N-methylphosphoramidobromidate (868738-72-1) + 4-(3-hydroxypropyl)-2,6-di-tert-butylphenol (36294-23-2) → 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate (868738-76-5)

Guidance literature:

With pyridine; In benzene; at 40 ℃; for 2h;

DOI:10.1007/s11176-005-0172-7

Reference yield:

1-octadecanol (112-92-5) → 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate (868738-76-5)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 1.5 h / 80 - 85 °C

2: 2.17 g / Br₂ / benzene / 0.17 h / -5 °C

3: 51 percent / pyridine / benzene / 2 h / 40 °C

With pyridine; bromine; In benzene;

DOI:10.1007/s11176-005-0172-7

Reference yield:

C26H57N2OP (868738-71-0) → 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl octadecyl N-(2-bromoethyl)-N-methylphosphoramidate (868738-76-5)

Guidance literature:

Multi-step reaction with 3 steps

1: dioxane / 75 - 85 °C

2: 2.17 g / Br₂ / benzene / 0.17 h / -5 °C

3: 51 percent / pyridine / benzene / 2 h / 40 °C

With pyridine; bromine; In 1,4-dioxane; benzene;

DOI:10.1007/s11176-005-0172-7

upstream raw materials:

octadecyl N-(2-bromoethyl)-N-methylphosphoramidobromidate

4-(3-hydroxypropyl)-2,6-di-tert-butylphenol

C₂₆H₅₇N₂OP

1-octadecanol