dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

Base Information

Chemical Name:dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate
CAS No.:1242096-24-7
Molecular Formula:C₁₉H₂₅ClO₅
Molecular Weight:368.858
Hs Code.:

Synonyms:dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

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Chemical Property of dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

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Technology Process of dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

There total 2 articles about dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7560-44-3,20754-21-6,20754-24-9
methyl 4-chlorocinnamate

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 1242096-24-7
dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

Guidance literature:: methyl 4-chlorocinnamate; 1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; methanol; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 0.5h;
DOI:10.1039/c0cc01110j

Reference yield: 74.0%

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 1242096-10-1
dimethyl 3-(4-chlorophenyl)-2,2-dimethylpentane-1,5-dioate

: 1242096-24-7
dimethyl 3-(4-chlorophenyl)-2,2,6,6-tetramethyl-5-oxo-heptane-1,7-dioate

Guidance literature:: With iron(II) bromide; In 1,2-dichloro-ethane; at 110 ℃; for 20h; optical yield given as %de; stereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c0cc01182g