2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

Base Information

Chemical Name:2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine
CAS No.:439557-48-9
Molecular Formula:C₃₂H₃₂N₂O₄
Molecular Weight:508.617
Hs Code.:

Synonyms:2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

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Chemical Property of 2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

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Technology Process of 2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

There total 4 articles about 2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 439571-76-3
2-phenyl-4-(N-{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl})aminomethyl-3-butylpyridine

: 439557-48-9
2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

Guidance literature:: piperonal; 2-phenyl-4-(N-{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl})aminomethyl-3-butylpyridine; In 1,2-dichloro-ethane; for 3h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane;

With ammonia; water; In 1,2-dichloro-ethane;

Reference yield:

: 5-butyl-4-phenyl-oxazole

: 439557-48-9
2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 0.5 h / 100 °C

2: lithium aluminium tetrahydride / tetrahydrofuran

3: thionyl chloride / chloroform / 2 h / 50 °C

4: potassium carbonate / DMF (N,N-dimethyl-formamide) / 3 h / Heating / reflux

5: 1,2-dichloro-ethane / 3 h

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); chloroform; 1,2-dichloro-ethane;

Reference yield:

: 439571-75-2
2-phenyl-4-hydroxymethyl-3-butylpyridine

: 439557-48-9
2-phenyl-4-(N,N-di{2H-benzo[3,4-d]-1,3-dioxolan-5-ylmethyl}amino)methyl-3-butylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / chloroform / 2 h / 50 °C

2: potassium carbonate / DMF (N,N-dimethyl-formamide) / 3 h / Heating / reflux

3: 1,2-dichloro-ethane / 3 h

With thionyl chloride; potassium carbonate; In DMF (N,N-dimethyl-formamide); chloroform; 1,2-dichloro-ethane;