BROMODICHLOROACETICACID

Base Information

Chemical Name:BROMODICHLOROACETICACID
CAS No.:71333-14-7
Molecular Formula:C₂₁H₂₇NO₄
Molecular Weight:357.45
Hs Code.:
Mol file:71333-14-7.mol

Synonyms:14β-Ethylmorphinon-dimethylacetal;(+-)-14-ethyl-morphinone dimethyl acetal;

Suppliers and Price of BROMODICHLOROACETICACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of BROMODICHLOROACETICACID

Chemical Property:

PSA：51.16000
LogP:2.54440

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BROMODICHLOROACETICACID

There total 4 articles about BROMODICHLOROACETICACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71333-03-4
(17R)-4,5α-epoxy-3,6,6-trimethoxy-17-methyl-14,17-ethano-morphin-7-enium; iodide

: 71333-14-7
14β-Ethylmorphinon-dimethylacetal

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; for 4h;
DOI:10.1002/cber.19791120722

Reference yield:

: 32398-36-0
4,5α-epoxy-3,6,6-trimethoxy-17-methyl-morphin-8(14)-en-7β-ol

: 71333-14-7
14β-Ethylmorphinon-dimethylacetal

Guidance literature:: Multi-step reaction with 4 steps

1: xylene / 12 h / Heating

2: LiAlH₄ / diethyl ether / 3 h / Heating

3: methanol / 1 h / Ambient temperature

4: Li3H> / tetrahydrofuran / 4 h

With lithium aluminium tetrahydride; lithium triethylborohydride; In tetrahydrofuran; methanol; diethyl ether; xylene;
DOI:10.1002/cber.19791120722

Reference yield:

: 71333-21-6
[2-(4,5α-epoxy-3,6,6-trimethoxy-17-methyl-morphin-7-en-14-yl)-ethyl]-dimethyl-amine

: 71333-14-7
14β-Ethylmorphinon-dimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / Ambient temperature

2: Li3H> / tetrahydrofuran / 4 h

With lithium triethylborohydride; In tetrahydrofuran; methanol;
DOI:10.1002/cber.19791120722