C₁₈H₁₈O₅

Base Information

Chemical Name:C₁₈H₁₈O₅
CAS No.:1163751-08-3
Molecular Formula:C₁₈H₁₈O₅
Molecular Weight:314.338
Hs Code.:

C<sub>18</sub>H<sub>18</sub>O<sub>5</sub>

Synonyms:C₁₈H₁₈O₅

Suppliers and Price of C₁₈H₁₈O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₈O₅

Chemical Property:

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Technology Process of C₁₈H₁₈O₅

There total 12 articles about C₁₈H₁₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1163751-07-2
C₁₈H₂₀O₅

: 1163751-08-3
C₁₈H₁₈O₅

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 25 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.200900264 DOI:10.1021/ja1048994

Reference yield:

: 533-31-3
Sesamol

: 1163751-08-3
C₁₈H₁₈O₅

Guidance literature:: Multi-step reaction with 11 steps

1: Inert atmosphere

2: n-butyllithium / Inert atmosphere

3: hydrogenchloride / ethanol; water / Inert atmosphere

4: acetic acid / Inert atmosphere

5: potassium carbonate / Inert atmosphere

6: potassium tert-butylate / Inert atmosphere

7: AD-mix-β; water / Inert atmosphere

8: triethylamine / Inert atmosphere

9: sodium hydride / Inert atmosphere

10: triethylsilane; dichloro-acetic acid / Inert atmosphere

11: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere

With hydrogenchloride; triethylsilane; dichloro-acetic acid; n-butyllithium; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; In ethanol; water; 4: Duff reaction / 7: Sharpless dihydroxylation / 11: Swern oxidation;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 187040-02-4
5-methoxy methoxy-4-methyl benzo[d][1,3]dioxole

: 1163751-08-3
C₁₈H₁₈O₅

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogenchloride / ethanol; water / Inert atmosphere

2: acetic acid / Inert atmosphere

3: potassium carbonate / Inert atmosphere

4: potassium tert-butylate / Inert atmosphere

5: AD-mix-β; water / Inert atmosphere

6: triethylamine / Inert atmosphere

7: sodium hydride / Inert atmosphere

8: triethylsilane; dichloro-acetic acid / Inert atmosphere

9: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere

With hydrogenchloride; triethylsilane; dichloro-acetic acid; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; In ethanol; water; 2: Duff reaction / 5: Sharpless dihydroxylation / 9: Swern oxidation;
DOI:10.1016/j.tet.2011.04.094