Technology Process of C55H90BrNO11Si2
There total 49 articles about C55H90BrNO11Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
diethyl ether; acetonitrile;
at -47 ℃;
for 36h;
DOI:10.1002/anie.200390321
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 93 percent / NaHMDS / tetrahydrofuran / 5 h / -78 - 20 °C
2.1: 98 percent / Me2BBr / CH2Cl2; dimethyl ether / 1.5 h / -78 °C
3.1: 82 percent / TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 24 h / 20 °C
4.1: n-BuLi; Et2NH / hexane; tetrahydrofuran / 0.2 h / -78 °C
4.2: hexane; tetrahydrofuran / 0.5 h / -78 °C
5.1: pyridine / acetonitrile; diethyl ether / 36 h / -47 °C
With
pyridine; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; dimethylboron bromide; 4 A molecular sieve; sodium hexamethyldisilazane; diethylamine;
In
tetrahydrofuran; diethyl ether; hexane; Dimethyl ether; dichloromethane; acetonitrile;
1.1: Julia reaction;
DOI:10.1039/b308305e
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 93 percent / NaHMDS / tetrahydrofuran / 5 h / -78 - 20 °C
2.1: 98 percent / Me2BBr / CH2Cl2; dimethyl ether / 1.5 h / -78 °C
3.1: 82 percent / TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 24 h / 20 °C
4.1: n-BuLi; Et2NH / hexane; tetrahydrofuran / 0.2 h / -78 °C
4.2: hexane; tetrahydrofuran / 0.5 h / -78 °C
5.1: pyridine / acetonitrile; diethyl ether / 36 h / -47 °C
With
pyridine; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; dimethylboron bromide; 4 A molecular sieve; sodium hexamethyldisilazane; diethylamine;
In
tetrahydrofuran; diethyl ether; hexane; Dimethyl ether; dichloromethane; acetonitrile;
1.1: Julia reaction;
DOI:10.1039/b308305e