(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

Base Information

Chemical Name:(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester
CAS No.:201815-23-8
Molecular Formula:C₁₁H₁₄O₅
Molecular Weight:226.229
Hs Code.:

Synonyms:(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

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Chemical Property of (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

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Technology Process of (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

There total 2 articles about (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 201815-23-8
(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

Guidance literature:: In tetrahydrofuran; at -30 ℃; for 144h;

Reference yield:

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 555-31-7
aluminum isopropoxide

: C₄₇H₃₆O₄^(2-)*2C₃H₇O^(1-)*Ti⁽⁴⁺⁾

: 201815-23-8
(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

: (1S,2R,3S,4R)-7-Oxa-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid monoisopropyl ester

Guidance literature:: In tetrahydrofuran; at -34 ℃; for 576h; Product distribution; other solvent, temperature, reaction time; also in absence of Al(i-PrO)3;
DOI:10.1021/jo971731t