S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

Base Information

Chemical Name:S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate
CAS No.:1314941-72-4
Molecular Formula:C₂₄H₂₉NO₁₁S
Molecular Weight:539.56
Hs Code.:

Synonyms:S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

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Chemical Property of S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

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Technology Process of S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

There total 5 articles about S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1162198-69-7,83800-17-3
(Z)-2-acetoxy-3-(3,4-diacetoxyphenyl)acrylic acid

: 172749-96-1
N-[(tert-butoxy)carbonyl]-L-cysteine methyl ester

: 1314941-72-4
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

Guidance literature:: (Z)-2-acetoxy-3-(3,4-diacetoxyphenyl)acrylic acid; N-[(tert-butoxy)carbonyl]-L-cysteine methyl ester; In dichloromethane; at 0 ℃; for 0.25h;

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.07.016

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1314941-72-4
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 6 h / Inert atmosphere

2.1: dichloromethane / 0.25 h / 0 °C

2.2: 3 h / 0 - 20 °C

With triethylamine; In dichloromethane;
DOI:10.1016/j.ejmech.2012.07.016

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 1314941-72-4
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) ((2-acetoxy)-3-(3,4-methylenedioxyphenyl))propenethioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate / 120 °C

2.1: hydrogenchloride / water / 100 °C

3.1: 6 h / 20 °C

4.1: dichloromethane / 0.25 h / 0 °C

4.2: 3 h / 0 - 20 °C

With hydrogenchloride; sodium acetate; In dichloromethane; water;
DOI:10.1016/j.ejmech.2012.07.016