C₂₃H₃₆O₆SSi

Base Information Edit

Chemical Name:C₂₃H₃₆O₆SSi
CAS No.:1380234-61-6
Molecular Formula:C₂₃H₃₆O₆SSi
Molecular Weight:468.687
Hs Code.:
Mol file:1380234-61-6.mol

C<sub>23</sub>H<sub>36</sub>O<sub>6</sub>SSi

Synonyms:C₂₃H₃₆O₆SSi

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Chemical Property of C₂₃H₃₆O₆SSi Edit

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Technology Process of C₂₃H₃₆O₆SSi

There total 6 articles about C₂₃H₃₆O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1380234-48-9
C₂₃H₃₄O₆SSi

: 1380234-61-6
C₂₃H₃₆O₆SSi

Guidance literature:: With L-Selectride; In tetrahydrofuran; dichloromethane; at -78 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1021/ol301090v

Reference yield:

: 58888-62-3
ethyl 6-O-tert-butyldimethylsilyl-4-hydroxyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 1380234-61-6
C₂₃H₃₆O₆SSi

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2: benzenesulfinic acid sodium salt; 18-crown-6 ether / tetrahydrofuran / 21 h / 20 °C / Inert atmosphere

3: L-Selectride / tetrahydrofuran; dichloromethane / 1.17 h / -78 °C / Inert atmosphere

With oxalyl dichloride; 18-crown-6 ether; benzenesulfinic acid sodium salt; L-Selectride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 1: Swern oxidation / 2: Padwa elimination;
DOI:10.1021/ol301090v

Reference yield:

: 23339-15-3
ethyl 2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 1380234-61-6
C₂₃H₃₆O₆SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 70 h / 0 - 20 °C / Inert atmosphere

2: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3: benzenesulfinic acid sodium salt; 18-crown-6 ether / tetrahydrofuran / 21 h / 20 °C / Inert atmosphere

4: L-Selectride / tetrahydrofuran; dichloromethane / 1.17 h / -78 °C / Inert atmosphere

With 1H-imidazole; oxalyl dichloride; 18-crown-6 ether; benzenesulfinic acid sodium salt; L-Selectride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: Swern oxidation / 3: Padwa elimination;
DOI:10.1021/ol301090v