bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

Base Information

Chemical Name:bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide
CAS No.:1311030-00-8
Molecular Formula:C₃₆H₂₈Cl₈N₂O₄S₂
Molecular Weight:900.385
Hs Code.:

Synonyms:bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

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Chemical Property of bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

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Technology Process of bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

There total 2 articles about bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1311029-98-7
2,8-di-(m,p-dichlorophenyl)-5-acetylthiomethyl-1-aza-3,7-dioxabicyclo[3.3.0]octane

: 1311029-85-2
2,8-di-(3,4-dichlorophenyl)-5-thiomethyl-1-aza-3,7-dioxabicyclo[3.3.0]octane

: 1311030-00-8
bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

Guidance literature:: With ammonia; In methanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo2008498

Reference yield:

: 6287-38-3
3,4-dichlorobenzaldehyde

: 1311030-00-8
bis-(2,8-di-(3,4-dichlorophenyl)-1-aza-3,7-dioxabicyclo[3.3.0]octane)-5-methyldisulfide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

2: triphenylphosphine; diethylazodicarboxylate / benzene / 0 °C / Reflux

3: ammonia / methanol / 0 - 20 °C / Inert atmosphere

With ammonia; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In methanol; toluene; benzene; 2: Mitsunobu reaction;
DOI:10.1021/jo2008498