3-CHLORO-4-NITROBENZENESULFONYL CHLORIDE

Base Information

• Chemical Name: 3-CHLORO-4-NITROBENZENESULFONYL CHLORIDE
• CAS No.: 64835-30-9
• Molecular Formula: C6H3 Cl2 N O4 S
• Molecular Weight: 256.066
• Hs Code.: 2904909090

Synonyms:3-Chloro-4-nitro-benzenesulfonylchloride

Chemical Property of 3-CHLORO-4-NITROBENZENESULFONYL CHLORIDE

Chemical Property:

• Vapor Pressure: 7.31E-06mmHg at 25°C
• Melting Point: 36-39°C
• Refractive Index: 1.599
• Boiling Point: 387.5°C at 760 mmHg
• Flash Point: 188.2°C
• PSA: 88.34000
• Density: 1.708g/cm³
• LogP: 3.77970
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Sensitive.: Moisture Sensitive
• Water Solubility.: Reacts with water.

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-4-nitrobenzene-1-sulfonyl chloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Chloro-4-nitrobenzenesulfonyl chloride is the reactant in the synthesis of aminobenzenesulfonyl fluorides. 3-Chloro-4-nitrobenzenesulfonyl chloride is also used as intermediates in organic synthesis.

Technology Process of 3-CHLORO-4-NITROBENZENESULFONYL CHLORIDE

There total 1 articles about 3-CHLORO-4-NITROBENZENESULFONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-chloro-4-nitro-benzenesulfonyl chloride (64835-30-9)

Guidance literature:

Reference yield: 87.5%

3-chloro-4-nitro-benzenesulfonyl chloride (64835-30-9) + 4-amino-o-xylene (95-64-7) → 3-chloro-N-(3,4-dimethylphenyl)-4-nitrobenzenesulfonamide

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.jmedchem.0c00932

Reference yield: 85.0%

3-Hydroxy-cumarin (939-19-5) + 3-chloro-4-nitro-benzenesulfonyl chloride (64835-30-9) → 2-oxo-2H-chromen-3-yl 3-chloro-4-nitrobenzenesulfonate

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/j.bioorg.2016.09.006

Downstream raw materials:

(S)-2-[(3-Chloro-4-nitro-benzenesulfonyl)-(4-nitro-benzyl)-amino]-propionic acid

[(3-chloro-4-nitro-benzenesulfonyl)-(4-nitro-benzyl)-amino]-acetic acid

(S)-2-(3-Chloro-4-nitro-benzenesulfonylamino)-3-methyl-butyric acid

(S)-2-[Benzyl-(3-chloro-4-nitro-benzenesulfonyl)-amino]-3-methyl-butyric acid

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