(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

Base Information

Chemical Name:(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate
CAS No.:1610376-82-3
Molecular Formula:C₁₇H₂₇O₃PS₂
Molecular Weight:374.505
Hs Code.:

Synonyms:(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

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Technology Process of (E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

There total 3 articles about (E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1610376-66-3
2-phenethyl-2-(prop-1-en-2-yl)oxirane

: 298-06-6
O,O-Diethyl hydrogen phosphorodithioate

: 1610376-75-4
(Z)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

: 1610376-82-3
(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

Guidance literature:: In toluene; at 20 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 60550-54-1
2-methyl-5-phenylpent-1-en-3-one

: 1610376-75-4
(Z)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

: 1610376-82-3
(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; diethyl ether / 0.37 h / -100 °C / Inert atmosphere

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

3: toluene / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: C₁₃H₁₇ClO

: 1610376-75-4
(Z)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

: 1610376-82-3
(E)-S-(3-(hydroxymethyl)-2-methyl-5-phenylpent-2-en-1-yl) O,O-diethylphosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

2: toluene / 20 °C / Inert atmosphere

With sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028