C₃₃H₂₅BF₂N₂O₅

Base Information

Chemical Name:C₃₃H₂₅BF₂N₂O₅
CAS No.:1300036-86-5
Molecular Formula:C₃₃H₂₅BF₂N₂O₅
Molecular Weight:578.38
Hs Code.:

C<sub>33</sub>H<sub>25</sub>BF<sub>2</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₃H₂₅BF₂N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₅BF₂N₂O₅

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Technology Process of C₃₃H₂₅BF₂N₂O₅

There total 6 articles about C₃₃H₂₅BF₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1300036-85-4
C₃₇H₃₅BF₂N₂O₅Si

: 1300036-86-5
C₃₃H₂₅BF₂N₂O₅

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; water; at 25 ℃; for 24h;
DOI:10.1016/j.bmcl.2011.01.040

Reference yield:

: C₃₂H₂₇IN₂O₅

: 1300036-86-5
C₃₃H₂₅BF₂N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate; triethylamine / 1,2-dichloro-ethane / Inert atmosphere; Reflux

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / dichloromethane / 24 h / 25 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol; water / 24 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; 2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.01.040

Reference yield:

: 69640-32-0
2-(2-methoxyphenyl)pyrrole

: 1300036-86-5
C₃₃H₂₅BF₂N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 25 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: boron trifluoride diethyl etherate; triethylamine / 1,2-dichloro-ethane / Inert atmosphere; Reflux

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / dichloromethane / 24 h / 25 °C / Inert atmosphere

4.1: potassium carbonate / tetrahydrofuran; methanol; water / 24 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; potassium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; 3.1: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.01.040