C₄₄H₄₅N₇O₆

Base Information

Chemical Name:C₄₄H₄₅N₇O₆
CAS No.:1357259-18-7
Molecular Formula:C₄₄H₄₅N₇O₆
Molecular Weight:767.885
Hs Code.:

C<sub>44</sub>H<sub>45</sub>N<sub>7</sub>O<sub>6</sub>

Synonyms:C₄₄H₄₅N₇O₆

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Chemical Property of C₄₄H₄₅N₇O₆

Chemical Property:

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Technology Process of C₄₄H₄₅N₇O₆

There total 12 articles about C₄₄H₄₅N₇O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₃₄N₆O₃*(x)ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1357259-18-7
C₄₄H₄₅N₇O₆

Guidance literature:: N-methoxycarbonyl-L-valine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 10 ℃; for 1h;

C₃₇H₃₄N₆O₃*(x)ClH; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 10 ℃; for 48h;

Reference yield:

: 135484-83-2
2-amino-4-bromo-benzoic acid methyl ester

: 1357259-18-7
C₄₄H₄₅N₇O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 3 h / 50 °C

1.2: pH 2

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 15 h / 20 °C

3.1: sodium hydroxide / water; tetrahydrofuran / 1 h / 20 °C

4.1: potassium hydroxide / ethanol; water / 3 h / 80 °C

4.2: 0 °C / pH 7

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 90 °C / Inert atmosphere

5.2: pH 10

6.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 1 h / 10 °C

7.2: 48 h / 0 - 10 °C

With hydrogenchloride; water; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 112253-70-0
2-amino-4-bromobenzamide

: 1357259-18-7
C₄₄H₄₅N₇O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water; tetrahydrofuran / 1 h / 20 °C

2.1: potassium hydroxide / ethanol; water / 3 h / 80 °C

2.2: 0 °C / pH 7

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 90 °C / Inert atmosphere

3.2: pH 10

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 1 h / 10 °C

5.2: 48 h / 0 - 10 °C

With hydrogenchloride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene; acetonitrile;