dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

Base Information

Chemical Name:dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer
CAS No.:1351363-35-3
Molecular Formula:C₄₂H₄₂Cl₄Rh₂
Molecular Weight:894.418
Hs Code.:

Synonyms:dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

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Chemical Property of dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

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Technology Process of dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

There total 2 articles about dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.2%

: 3-biphenyl-1 ,2,4,5-tetramethyl-1,3-cyclopentadiene

: rhodium(III) trichloride hydrate

: 1351363-35-3
dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

Guidance literature:: In methanol; at 69.84 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.jinorgbio.2015.10.008

Reference yield: 32.34%

: rhodium(III) chloride

: 3-biphenyl-1 ,2,4,5-tetramethyl-1,3-cyclopentadiene

: 1351363-35-3
dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

Guidance literature:: In methanol; at 69.84 ℃; for 48h; Inert atmosphere;

Reference yield: 99.0%

: ammonium hexafluorophosphate

: 1351363-35-3
dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer

: N-(5,6-dimethoxypyrimidin-4-yl)-4-((isoquinolin-3-ylmethylene)-amino)benzenesulfonamide (2-quinolyliminesulfdoxine)

: C₄₃H₄₀ClN₅O₄RhS⁽¹⁺⁾*F₆P^(1-)

Guidance literature:: dichloro(4-(tetramethylcyclopentadienyl)-1,1'-biphenyl)rhodium(III)dimer; N-(5,6-dimethoxypyrimidin-4-yl)-4-((isoquinolin-3-ylmethylene)-amino)benzenesulfonamide (2-quinolyliminesulfdoxine); In methanol; at 20 ℃; for 16h;

ammonium hexafluorophosphate; In methanol; acetone; at 20 ℃; for 2h;
DOI:10.1002/chem.201801090