3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

Base Information

Chemical Name:3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure
CAS No.:107223-11-0
Molecular Formula:C₂₉H₃₄N₄O₁₀
Molecular Weight:598.61
Hs Code.:

Synonyms:3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

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Chemical Property of 3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

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Technology Process of 3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

There total 8 articles about 3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 107223-10-9
3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

: 107223-11-0
3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 2h;

Reference yield:

: 107244-49-5
3-O-Benzyl-6-(benzyloxycarbonylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

: 107223-11-0
3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 0.1N HCl, H₂ / 10percent Pd/C / methanol / 1.5 h

2: 78 percent / NaHCO₃ / tetrahydrofuran; H₂O / 18 h / 0 deg C to room temp.

3: 81 percent / 1N KOH,H₂O / methanol / 5 h / 0 °C

4: 98 percent / trifluoroacetic acid / 2 h / 0 °C

With hydrogenchloride; potassium hydroxide; hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; water;

Reference yield:

: 107223-06-3
2,5-Di-O-acetyl-3-O-benzyl-6-(benzyloxycarbonylamino)-1,6-didesoxy-1-<3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

: 107223-11-0
3-O-Benzyl-6-(O-benzyl-L-serylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / methanol; diethyl ether

2: 98 percent / 1M MeONa / methanol / 5 h / Ambient temperature

3: 89 percent / 0.1N HCl, H₂ / 10percent Pd/C / methanol / 1.5 h

4: 78 percent / NaHCO₃ / tetrahydrofuran; H₂O / 18 h / 0 deg C to room temp.

5: 81 percent / 1N KOH,H₂O / methanol / 5 h / 0 °C

6: 98 percent / trifluoroacetic acid / 2 h / 0 °C

With hydrogenchloride; potassium hydroxide; hydrogen; sodium methylate; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; water;