Technology Process of C45H58N4O8SSi
There total 4 articles about C45H58N4O8SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C35H36N4O7S;
With
di-tert-butyltin dichloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.25h;
Inert atmosphere;
Reflux;
chloromethoxy-triisopropyl-silane;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja206095a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine / 3 h / 20 °C / Inert atmosphere
2.1: di-tert-butyltin dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / Inert atmosphere; Reflux
2.2: 20 °C / Inert atmosphere
With
di-tert-butyltin dichloride; N-ethyl-N,N-diisopropylamine;
In
pyridine; dichloromethane;
DOI:10.1021/ja206095a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanol; N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2.1: pyridine / 3 h / 20 °C / Inert atmosphere
3.1: di-tert-butyltin dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / Inert atmosphere; Reflux
3.2: 20 °C / Inert atmosphere
With
di-tert-butyltin dichloride; N-ethyl-N,N-diisopropylamine;
In
pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja206095a