6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

Base Information

Chemical Name:6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole
CAS No.:859871-38-8
Molecular Formula:C₂₃H₃₃NO₂Si₂
Molecular Weight:411.692
Hs Code.:

6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1<i>H</i>-indole

Synonyms:6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

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Chemical Property of 6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

Chemical Property:

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Technology Process of 6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

There total 2 articles about 6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859871-33-3
5-(benzyloxy)-2-iodoaniline

: 58434-99-4
1-<(trimethylsilyl)oxy>-4-(trimethylsilyl)-3-butyne

: 859871-38-8
6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

Guidance literature:: With potassium carbonate; triphenylphosphine; lithium chloride; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1055/s-2005-868485

Reference yield:

: 183007-32-1
4-benzyloxy-1-iodo-2-nitrobenzene

: 859871-38-8
6-benzyloxy-2-trimethylsilanyl-3-(2-trimethylsilanyloxy-ethyl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / H₂NNH₂; FeCl₃*H₂O; activated charcoal / methanol / 38 h / Heating

2: LiCl; PPh₃; K₂CO₃ / Pd(OAc)2 / dimethylformamide / 2 h / 80 °C

With iron(III) chloride; potassium carbonate; pyrographite; triphenylphosphine; lithium chloride; hydrazine; palladium diacetate; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-868485