S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

Base Information

Chemical Name:S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate
CAS No.:1314941-70-2
Molecular Formula:C₂₂H₂₉NO₉S
Molecular Weight:483.54
Hs Code.:

Synonyms:S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

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Chemical Property of S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

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Technology Process of S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

There total 5 articles about S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1162198-69-7,83800-17-3
(Z)-2-acetoxy-3-(3,4-diacetoxyphenyl)acrylic acid

: 1314941-70-2
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 10% Pd/C; hydrogen / methanol / 24 h / 20 °C / 11400.8 Torr

2.1: dichloromethane / 0.25 h / 0 °C

2.2: 3 h / 0 - 20 °C

With 10% Pd/C; hydrogen; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2012.07.016

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1314941-70-2
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 6 h / Inert atmosphere

2.1: dichloromethane / 0.25 h / 0 °C

2.2: 3 h / 0 - 20 °C

With triethylamine; In dichloromethane;
DOI:10.1016/j.ejmech.2012.07.016

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 1314941-70-2
S-((R)-3-methoxy-3-oxo-2-(tert-butoxycarbonylamino)propyl) 3-(3,4-diacetoxyphenyl)propanethioate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium acetate / 120 °C

2.1: hydrogenchloride / water / 100 °C

3.1: 6 h / 20 °C

4.1: 10% Pd/C; hydrogen / methanol / 24 h / 20 °C / 11400.8 Torr

5.1: dichloromethane / 0.25 h / 0 °C

5.2: 3 h / 0 - 20 °C

With hydrogenchloride; 10% Pd/C; hydrogen; sodium acetate; In methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.07.016