(2R,3R)-2,3-epoxy decanal

Base Information

Chemical Name:(2R,3R)-2,3-epoxy decanal
CAS No.:1308381-98-7
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:

Synonyms:(2R,3R)-2,3-epoxy decanal

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Chemical Property of (2R,3R)-2,3-epoxy decanal

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Technology Process of (2R,3R)-2,3-epoxy decanal

There total 5 articles about (2R,3R)-2,3-epoxy decanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 107796-95-2
((2R,3R)-3-heptyloxiran-2-yl)methanol

: 1308381-98-7,102369-06-2
(2R,3R)-2,3-epoxy decanal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2016.12.008

Reference yield:

: 3913-81-3
(E)-2-decenal

: 1048958-35-5,102369-06-2
2,3-EPOXYDECANAL

: 1308381-98-7,102369-06-2
(2R,3R)-2,3-epoxy decanal

Guidance literature:: With (S)-α,α-bis(4-hexylphenylthio)-2-pyrrolidinemethanol trimethylsilylether; dihydrogen peroxide; In ethanol; water; at 20 ℃; for 16h; Green chemistry;
DOI:10.1039/c2ob26247a

Reference yield:

: 629-04-9
1-Bromoheptane

: 1308381-98-7,102369-06-2
(2R,3R)-2,3-epoxy decanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; hexane / 3 h / -78 - -30 °C / Inert atmosphere

1.2: 24.5 h / -30 - 20 °C / Inert atmosphere

2.1: hydrogen; sodium tetrahydroborate; nickel(II) acetate tetrahydrate; ethylenediamine / ethanol / 6 h

3.1: tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; titanium(IV) isopropylate / dichloromethane; decane / 72 h / -23 - -10 °C / Inert atmosphere; Molecular sieve

4.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; n-butyllithium; diethyl (2R,3R)-tartrate; hydrogen; nickel(II) acetate tetrahydrate; Dess-Martin periodane; ethylenediamine; In tetrahydrofuran; decane; ethanol; hexane; dichloromethane; 3.1: |Sharpless Asymmetric Epoxidation / 4.1: |Dess-Martin Oxidation;
DOI:10.1016/j.tetasy.2016.12.008