C₁₃H₁₈NI

Base Information

• Chemical Name: C₁₃H₁₈NI
• CAS No.: 960119-51-1
• Molecular Formula: C₁₃H₁₈IN
• Molecular Weight: 315.197
• Mol file: 960119-51-1.mol

Synonyms:C₁₃H₁₈NI

Chemical Property of C₁₃H₁₈NI

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₃H₁₈NI

There total 1 articles about C₁₃H₁₈NI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-iodophenylamine (615-43-0) + cyclohexanecarbaldehyde (2043-61-0) → C13H18NI (960119-51-1)

Guidance literature:

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In ethyl acetate; at 20 ℃;

DOI:10.1021/ol7020737

Reference yield: 65.0%

(3aS,4R,6R,6aS)-4-chloro-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxole (6160-67-4,16136-64-4,17087-84-2,33823-06-2,57819-53-1,67253-98-9,72258-31-2,142034-31-9) + C13H18NI (960119-51-1) + C14H14O2S → C27H37NO5

Guidance literature:

With trifuran-2-yl-phosphane; palladium diacetate; caesium carbonate; In 1,4-dioxane; at 90 - 150 ℃; for 36h; regioselective reaction;

DOI:10.1039/d1sc03569j

Reference yield:

C13H18NI (960119-51-1) + cinnamamide (621-79-4,22031-64-7) → C22H26N2O

Guidance literature:

With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 110 ℃; for 17h;

DOI:10.1021/ol7020737

upstream raw materials:

2-iodophenylamine

cyclohexanecarbaldehyde

Refernces

• 1、 Zheng, Nan,Buchwald, Stephen L.. "Copper-catalyzed regiospecific synthesis of N-alkylbenzimidazoles". . p. 4749 - 4751. Retrieved 2008/03/14.