Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

Base Information

Chemical Name:Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine
CAS No.:148613-92-7
Molecular Formula:C₂₇H₃₀N₂O₄S
Molecular Weight:478.612
Hs Code.:

Synonyms:Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

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Chemical Property of Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

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Technology Process of Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

There total 4 articles about Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-59-9
p-toluenesulfonyl chloride

: 148613-91-6
Benzyl-[2-(6,7-dimethoxy-1H-indol-3-yl)-ethyl]-methyl-amine

: 148613-92-7
Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

Guidance literature:: With sodium hydroxide; cetyltrimethylammonim bromide; In dichloromethane; at 25 ℃; for 12h;
DOI:10.1016/S0040-4039(00)60427-6

Reference yield:

: 31165-13-6
6,7-dimethoxy-1H-indole

: 148613-92-7
Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / diethyl ether / 1 h / 0 °C

2: 96 percent / H₂O / 3 h / 25 °C

3: 96 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 4 h / Heating

4: 90 percent / NaOH / CTAB / CH₂Cl₂ / 12 h / 25 °C

With sodium hydroxide; lithium aluminium tetrahydride; cetyltrimethylammonim bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4039(00)60427-6

Reference yield:

: 75909-70-5
cloruro dell'acido 6,7-dimetossindol-3-gliossilico

: 148613-92-7
Benzyl-{2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl}-methyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂O / 3 h / 25 °C

2: 96 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 4 h / Heating

3: 90 percent / NaOH / CTAB / CH₂Cl₂ / 12 h / 25 °C

With sodium hydroxide; lithium aluminium tetrahydride; cetyltrimethylammonim bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4039(00)60427-6