C₅₁H₆₀Cl₃NO₂₄S

Base Information

Chemical Name:C₅₁H₆₀Cl₃NO₂₄S
CAS No.:1603850-56-1
Molecular Formula:C₅₁H₆₀Cl₃NO₂₄S
Molecular Weight:1209.45
Hs Code.:

C<sub>51</sub>H<sub>60</sub>Cl<sub>3</sub>NO<sub>24</sub>S

Synonyms:C₅₁H₆₀Cl₃NO₂₄S

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Chemical Property of C₅₁H₆₀Cl₃NO₂₄S

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Technology Process of C₅₁H₆₀Cl₃NO₂₄S

There total 7 articles about C₅₁H₆₀Cl₃NO₂₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1603850-44-7
ethyl [4,6-di-O-acetyl-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranosyl]-(1→4)-3,6-di-O-acetyl-2-deoxy-2-phthalimide-1-thio-β-D-glucopyranoside

: 3,4-di-O-acetyl-2-O-p-methoxybenzyl-L-fucipyranosyl-(N-phenyl)-2,2,2-trifluoroacetimidate

: 1603850-56-1
C₅₁H₆₀Cl₃NO₂₄S

Guidance literature:: ethyl [4,6-di-O-acetyl-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranosyl]-(1→4)-3,6-di-O-acetyl-2-deoxy-2-phthalimide-1-thio-β-D-glucopyranoside; 3,4-di-O-acetyl-2-O-p-methoxybenzyl-L-fucipyranosyl-(N-phenyl)-2,2,2-trifluoroacetimidate; With cyclopentyl methyl ether; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -80 ℃; for 5.5h; Molecular sieve; Inert atmosphere;
DOI:10.3390/molecules19010414

Reference yield:

: 1603850-36-7
ethyl (4,6-di-O-acetyl-β-D-galactopyranosyl)-(1→4)-3,6-di-O-acetyl-2-deoxy-2-phthalimide-1-thio-β-D-glucopyranoside

: 1603850-56-1
C₅₁H₆₀Cl₃NO₂₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: dibutyltin chloride / acetone / 0.17 h / 20 °C / Inert atmosphere

1.2: 0.33 h / 20 °C / Inert atmosphere

2.1: cyclopentyl methyl ether / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 5.5 h / -80 °C / Molecular sieve; Inert atmosphere

With cyclopentyl methyl ether; dibutyltin chloride; In dichloromethane; acetone;
DOI:10.3390/molecules19010414

Reference yield:

: 254444-74-1
ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1→4)-3,6-di-O-acetyl-2-deoxy-2-phthalimide-1-thio-β-D-glucopyranoside

: 1603850-56-1
C₅₁H₆₀Cl₃NO₂₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / methanol; dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2.1: camphor-10-sulfonic acid / methanol / 20 h / Reflux; Inert atmosphere

3.1: dmap / pyridine / 1 h / 0 - 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / water / 2 h / 0 - 20 °C / Inert atmosphere

5.1: dibutyltin chloride / acetone / 0.17 h / 20 °C / Inert atmosphere

5.2: 0.33 h / 20 °C / Inert atmosphere

6.1: cyclopentyl methyl ether / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

6.2: 5.5 h / -80 °C / Molecular sieve; Inert atmosphere

With dmap; cyclopentyl methyl ether; camphor-10-sulfonic acid; dibutyltin chloride; sodium methylate; trifluoroacetic acid; In pyridine; methanol; dichloromethane; water; acetone;
DOI:10.3390/molecules19010414