(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

Base Information

Chemical Name:(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid
CAS No.:1455088-34-2
Molecular Formula:C₂₇H₂₁N₃O₅
Molecular Weight:467.481
Hs Code.:

Synonyms:(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

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Chemical Property of (S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

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Technology Process of (S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

There total 2 articles about (S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1455093-14-7
(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid tert-butyl ester

: 1455088-34-2
(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 1455091-23-2
1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxylic acid methyl ester

: 120686-17-1
(S)-3-amino-4-phenylbutyric acid tert-butyl ester

: 1455088-34-2
(S)-3-[(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carbonyl)amino]-4-phenylbutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2-methoxy-ethanol / 1.5 h / Reflux

2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Cooling with ice

With trifluoroacetic acid; In dichloromethane; 2-methoxy-ethanol;