Technology Process of C16H14N2O3S
There total 8 articles about C16H14N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
ethanol; ethyl acetate;
at 50 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 2 h / 90 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C
2.2: 2 h
3.1: osmium(VIII) oxide / water; 1,4-dioxane / 0.5 h / 20 °C
3.2: 3 h / 20 °C
4.1: caesium carbonate / ethyl acetate; ethanol / 2 h / 50 °C
With
osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium(0); sodium hydride; caesium carbonate;
In
1,4-dioxane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: osmium(VIII) oxide / water; 1,4-dioxane / 0.5 h / 20 °C
1.2: 3 h / 20 °C
2.1: caesium carbonate / ethyl acetate; ethanol / 2 h / 50 °C
With
osmium(VIII) oxide; caesium carbonate;
In
1,4-dioxane; ethanol; water; ethyl acetate;