4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide

Base Information

• Chemical Name: 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide
• CAS No.: 544708-59-0
• Molecular Formula: C₄₆H₅₃BrO₃
• Molecular Weight: 733.829

Synonyms:4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide

Chemical Property of 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide

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Technology Process of 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide

There total 1 articles about 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-[2-[2-[4-[4-ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy]ethoxy]ethoxy]benzyl alcohol (177609-56-2) → 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide (544708-59-0)

Guidance literature:

With phosphorus tribromide; In tetrahydrofuran; for 5h;

DOI:10.1021/ja037592g

Reference yield: 95.0%

4,4'-bipyridine (553-26-4) + 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide (544708-59-0) → 1-{4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]-ethoxy]ethoxy]benzyl}-4-(4'-pyridinyl)-pyridinium hexafluorophosphate

Guidance literature:

In toluene; acetonitrile; at 80 ℃;

DOI:10.1039/b209836a

Reference yield: 90.0%

[2,17]dibenzo-30-crown-10 (17455-25-3) + 4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]ethoxy]ethoxy]benzylbromide (544708-59-0) + 1-{4-[2-[2-[4-[4-ethylphenyl-bis{4-t-butylphenyl}methyl]phenoxy]-ethoxy]ethoxy]benzyl}-4-(4'-pyridinyl)-pyridinium hexafluorophosphate → 1,1'-bis-(4-(2-(2-(4-[bis{4-t-butylphenyl}-4-ethylphenylmethyl]-phenoxy)-ethoxy)-ethoxy)-benzyl)-4,4'-bipyridinium*bis-para-phenylene-34-crown-10 rotaxane bis(hexafluorophosphate)

Guidance literature:

In benzonitrile; at 20 ℃;

DOI:10.1039/b209836a

upstream raw materials:

4-[2-[2-[4-[4-ethylphenyl-bis(4-tert-butylphenyl)methyl]phenoxy]ethoxy]ethoxy]benzyl alcohol

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