methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate

Base Information

• Chemical Name: methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate
• CAS No.: 1155918-08-3
• Molecular Formula: C₃₃H₃₄N₂O₇
• Molecular Weight: 570.642

Synonyms:methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate

Chemical Property of methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate

Chemical Property:

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Technology Process of methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate

There total 2 articles about methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 4-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)(2,4-dimethoxybenzyl)amino)-N-(2,4-dimethoxybenzyl)benzamido)benzoate (1219921-25-1) → methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate (1155918-08-3)

Guidance literature:

With diethylamine; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2009.12.137

Reference yield:

C33H32N2O7 → methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate (1155918-08-3)

Guidance literature:

With picoline-borane complex; at 20 ℃; for 14h;

DOI:10.1016/j.tetlet.2009.02.186

Reference yield: 77.0%

methyl 4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzoate (1155918-08-3) + 4-nitro-benzoic acid (62-23-7) → C40H37N3O10 (1155918-10-7)

Guidance literature:

With triethylamine; dichlorotriphenylphosphorane; In chloroform; for 14h; Reflux;

DOI:10.1016/j.tetlet.2009.02.186

upstream raw materials:

methyl 4-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)(2,4-dimethoxybenzyl)amino)-N-(2,4-dimethoxybenzyl)benzamido)benzoate

Downstream raw materials:

C₄₀H₃₇N₃O₁₀

methyl 4-(4-(4-((((9H-fluoren-9-yl)methoxy)cerbonyl)(2,4-dimethoxybenzyl)amino)-N-(2,4-dimethoxybenzyl)benzamido)-N-(2,4-dimethoxybenzyl)benzamido)benzoate

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