1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

Base Information

Chemical Name:1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone
CAS No.:859513-65-8
Molecular Formula:C₂₁H₂₈N₂O₅
Molecular Weight:388.464
Hs Code.:

Synonyms:1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

Suppliers and Price of 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

There total 1 articles about 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 859513-64-7
3-(4-methylphenyl)-2-(2-nitroethyl)pyrrole

: 127256-03-5
1,1,-dimethoxy-4-methyl-3-penten-2-one

: 859513-65-8
1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; Neat (no solvent);
DOI:10.1021/jo9025572

Reference yield: 54.0%

: 859513-65-8
1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

: 2,3-dihydro-1-(1,1-dimethoxymethyl)-3,3-dimethyl-7-(4-methylphenyl)dipyrrin

Guidance literature:: 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone; With sodium methylate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With hydrogenchloride; titanium(III) chloride; ammonium acetate; In tetrahydrofuran; water; at 20 ℃; for 6h; pH=6; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1021/jo9025572

Reference yield: 28.0%

: 859513-65-8
1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone

: 1-(1,1-dimethoxymethyl)-3,3-dimethyl-7-(4-methylphenyl)-2,3-dihydrodipyrrin

Guidance literature:: 1,1-dimethoxy-4,4-dimethyl-6-[3-(4-methylphenyl)pyrrol-2-yl]-5-nitro-2-hexanone; With sodium methylate; In tetrahydrofuran; at 20 ℃; for 1h;

With hydrogenchloride; titanium(III) chloride; ammonium acetate; In tetrahydrofuran; water; at 20 ℃; for 6h; pH=6.0; Further stages.;
DOI:10.1021/jo050467y