tri-2,6-xylyltin hydride

Base Information

Chemical Name:tri-2,6-xylyltin hydride
CAS No.:76681-91-9
Molecular Formula:C₂₄H₂₈Sn
Molecular Weight:435.196
Hs Code.:

Synonyms:tri-2,6-xylyltin hydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri-2,6-xylyltin hydride

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Technology Process of tri-2,6-xylyltin hydride

There total 1 articles about tri-2,6-xylyltin hydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1442462-84-1
tris(2,6-dimethylphenyl)tin(IV) bromide

: 76681-91-9
tri-2,6-xylyltin hydride

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h; Inert atmosphere; Cooling;
DOI:10.1139/cjc-2013-0503

Reference yield: 68.0%

: 76681-91-9
tri-2,6-xylyltin hydride

: 83183-33-9
Hexakis(2,6-dimethylphenyl)distannan

Guidance literature:: With α,alpha.'-azodiisobutyronitrile; In further solvent(s); AIBN in n-nonane was added to Sn compd. in n-nonane at 60°C for 1 h, mixture was refluxed for 3 h; mixture was cooled, colorless product was obtained, it was recrystd. from CHCl3 and MeOH; elem. anal.;

Reference yield: 52.0%

: 76681-91-9
tri-2,6-xylyltin hydride

: 65523-27-5
tri-2,6-xylyltin chloride

Guidance literature:: With tetrachloromethane; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; byproducts: CHCl3; a soln. of Sn-compound in CCl4 was heated at 90°C for 2 h in thepresence of AIBN; evapd., recrystd. from C6H6; elem. anal.;
DOI:10.1016/S0022-328X(00)81378-9