(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

Base Information

Chemical Name:(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate
CAS No.:1265917-44-9
Molecular Formula:C₂₁H₃₁NO₇
Molecular Weight:409.48
Hs Code.:

Synonyms:(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

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Technology Process of (2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

There total 1 articles about (2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: ethyl 2-acetyl-3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-methyl-4-nitrobutanoate

: 1265917-44-9
(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h;
DOI:10.1002/adsc.201000612

Reference yield:

: 1265917-44-9
(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

: C₁₉H₂₇NO₄

Guidance literature:: With 10% palladium on activated carbon; ammonium formate; In methanol; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201000612

Reference yield:

: 1265917-44-9
(2R,3R)-ethyl 3-[3-(cyclopentyloxy)-4-methoxyphenyl]-2-(1-hydroxyethyl)-2-methyl-4-nitrobutanoate

: C₁₉H₂₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; ammonium formate / methanol / 20 °C / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

With lithium aluminium tetrahydride; 10% palladium on activated carbon; ammonium formate; In tetrahydrofuran; methanol;
DOI:10.1002/adsc.201000612