3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile

Base Information

• Chemical Name: 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile
• CAS No.: 39889-31-1
• Molecular Formula: C₁₅H₁₁ClN₂O₂S
• Molecular Weight: 318.784

Synonyms:3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile

Chemical Property of 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile

Chemical Property:

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Technology Process of 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile

There total 5 articles about 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ⁶-benzo[1,4]thiazine-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-chloro-phenyl)-2-(2-nitro-benzenesulfonyl)-acrylonitrile (39889-23-1) → 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ6-benzo[1,4]thiazine-2-carbonitrile (39889-31-1)

Guidance literature:

With iron; In water; acetic acid;

Reference yield:

1-(cyanomethyl)sulfonyl-2-nitrobenzene (100559-85-1) → 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ6-benzo[1,4]thiazine-2-carbonitrile (39889-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₄OAc

2: Fe / acetic acid; H₂O

With ammonium acetate; iron; In water; acetic acid;

Reference yield:

sodium 2-nitrobenzenesulfinate (15898-45-0) → 3-(4-chloro-phenyl)-1,1-dioxo-1,2,3,4-tetrahydro-1λ6-benzo[1,4]thiazine-2-carbonitrile (39889-31-1)

Guidance literature:

Multi-step reaction with 3 steps

1: DMF

2: NH₄OAc

3: Fe / acetic acid; H₂O

With ammonium acetate; iron; N,N-dimethyl-formamide; In water; acetic acid;

upstream raw materials:

3-(4-chloro-phenyl)-2-(2-nitro-benzenesulfonyl)-acrylonitrile

1-(cyanomethyl)sulfonyl-2-nitrobenzene

sodium 2-nitrobenzenesulfinate

4-chlorobenzaldehyde

Downstream raw materials:

2-benzyl-3-(4-chlorophenyl)-2-cyano-3,4-dihydrobenzo[b]-1,4-thiazine 1,1-dioxide

3-(4-chlorophenyl)-2-cyano-2-methyl-3,4-dihydrobenzo[b]-1,4-thiazine 1,1-dioxide

3-(4-chlorophenyl)-2-cyano-2-ethyl-3,4-dihydrobenzo[b]-1,4-thiazine 1,1-dioxide

3-(4-chlorophenyl)-2-cyano-2-isopropyl-3,4-dihydrobenzo[b]-1,4-thiazine 1,1-dioxide

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