2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid

Base Information

• Chemical Name: 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid
• CAS No.: 86213-56-1
• Molecular Formula: C₁₆H₁₇N₆P*ClH
• Molecular Weight: 360.786

Synonyms:2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid

Chemical Property of 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid

Chemical Property:

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Technology Process of 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid

There total 4 articles about 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>iumchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N1-methylbenzamidrazone hydrochloride (28705-52-4) → 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ5-triazaphosphol>iumchlorid (86213-56-1)

Guidance literature:

With phosphorus pentachloride; In dichloromethane; 1.) 24 h, r.t., 2.) 24 h, reflux;

Reference yield: 87.0%

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ5,10λ5-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole (63148-50-5) + N1-methylbenzamidrazone hydrochloride (28705-52-4) → 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ5-triazaphosphol>iumchlorid (86213-56-1)

Guidance literature:

In dichloromethane; for 12h; Ambient temperature;

Reference yield:

2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ5-triazaphosphol> (86213-57-2) → 2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ5-triazaphosphol>iumchlorid (86213-56-1)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₅

2: 1 h / Ambient temperature

3: 87 percent / CH₂Cl₂ / 12 h / Ambient temperature

With phosphorus pentachloride; In dichloromethane;

upstream raw materials:

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ⁵,10λ⁵-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole

N¹-methylbenzamidrazone hydrochloride

1,6,6,6-Tetrachloro-2,10-dimethyl-4,8-diphenyl-2,3,5,7,9,10-hexaaza-1λ⁵,6λ⁵-diphospha-tricyclo[5.3.0.0^1,5]deca-3,8-diene

2',4'-Dihydro-2,2'-dimethyl-5,5'-diphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>

Downstream raw materials:

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ⁵,10λ⁵-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole

2',4'-Dihydro-2,2'-dimethyl-4',5,5'-triphenyl-2H-3,3'-spirobi<1,2,4,3λ⁵-triazaphosphol>

1,6-Dimethyl-3,8-diphenyl-9-trimethylsilanyl-1,2,4,6,7,9-hexaaza-5λ⁵-phospha-spiro[4.4]nona-2,4,7-triene

5,10-Dichlor-9,10-dihydro-1,9-dimethyl-3,7-diphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)

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