benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate

Base Information

• Chemical Name: benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate
• CAS No.: 1206874-31-8
• Molecular Formula: C₂₇H₂₈N₂O₅
• Molecular Weight: 460.53

Synonyms:benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate

Chemical Property of benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate

Chemical Property:

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Technology Process of benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate

There total 1 articles about benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

(S)-N-(benzyloxycarbonyl)valine (1149-26-4) + 2-hydroxy-N-(p-tolyl)benzamide (7164-80-9) → benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate (1206874-31-8)

Guidance literature:

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at -10 - 4 ℃; for 24h;

DOI:10.1016/j.tetlet.2009.10.084

Reference yield: 90.0%

benzyl (S)-1-((2-(p-tolylcarbamoyl)phenoxy)carbonyl)-2-methylpropylcarbamate (1206874-31-8) → (S)-1-(2-(4-methylphenylcarbamoyl)phenoxy)-3-methyl-1-oxobutan-2-aminium bromide (1206874-36-3)

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2009.10.084

upstream raw materials:

(S)-N-(benzyloxycarbonyl)valine

2-hydroxy-N-(p-tolyl)benzamide

Downstream raw materials:

(S)-1-(2-(4-methylphenylcarbamoyl)phenoxy)-3-methyl-1-oxobutan-2-aminium bromide

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