N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

Base Information

Chemical Name:N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester
CAS No.:35873-55-3
Molecular Formula:C₁₄H₂₄Cl₂N₂O₄
Molecular Weight:355.262
Hs Code.:

<i>N</i>,<i>N</i>'-<i>trans</i>-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

Synonyms:N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

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Chemical Property of N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

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Technology Process of N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

There total 1 articles about N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10029-07-9
trans-1,4-cyclohexane-bis(methylamine)

: 627-11-2
2-Chloroethyl chloroformate

: 35873-55-3
N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

Guidance literature:: With potassium carbonate; In acetone; Heating;
DOI:10.1021/jm00294a019

Reference yield:

: 35873-55-3
N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

: 35873-80-4
3,3'-trans-cyclohexane-1,4-diyldimethyl-bis-oxazolidin-2-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 20h;
DOI:10.1021/jm00294a019

Reference yield:

: 35873-55-3
N,N'-trans-cyclohexane-1,4-diyldimethyl-bis-carbamic acid bis-(2-chloro-ethyl) ester

: N_.N'-(2-bromethyl)-trans-1.4-cyclohexanbis-(methylamin)

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 20 h / 25 °C

2: HBr / acetic acid

With hydrogen bromide; sodium hydride; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00294a019