(3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine

Base Information

• Chemical Name: (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine
• CAS No.: 158109-52-5
• Molecular Formula: C₁₆H₂₄N₂O₃
• Molecular Weight: 292.378

Synonyms:(3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine

Chemical Property of (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine

Chemical Property:

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Technology Process of (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine

There total 2 articles about (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3S,6R)-2,5-Dimethoxy-6-isopropyl-3-<<4-<(trimethylsilyl)oxy>-3-cyclohexen-1-yl>methyl>-2,6-dihydro-1,4-pyrazine (137232-89-4,137330-21-3) → (3S,6R,1'S)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine + (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine (158109-52-5)

Guidance literature:

With p-benzoquinone; palladium diacetate; In acetonitrile; at 23 ℃; for 3.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00089a019

Reference yield:

(3S,6R)-2,5-Dimethoxy-6-isopropyl-3-<<4-<(trimethylsilyl)oxy>-3-cyclohexen-1-yl>methyl>-2,6-dihydro-1,4-pyrazine (137232-89-4,137330-21-3) → (3S,6R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-1-cyclohexyl)methyl>-3,6-dihydro-1,4-pyrazine (137232-88-3) + (3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine (158109-52-5)

Guidance literature:

With allyl methyl carbonate; palladium diacetate; In acetonitrile; for 3.5h; Yield given. Yields of byproduct given; Heating;

DOI:10.1021/jo00089a019

Reference yield:

(3S,6R,1'R)-2,5-Dimethoxy-6-isopropyl-3-<(4-oxo-2-cyclohexen-1-yl)methyl>-3,6-dihydro-1,4-pyrazine (158109-52-5) → (R)-4-((2S,5R)-5-Isopropyl-3,6-dimethoxy-2,5-dihydro-pyrazin-2-ylmethyl)-cyclohex-2-enol (1026811-57-3)

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride; In methanol; for 0.25h;

DOI:10.1021/jo00089a019

upstream raw materials:

(3S,6R)-2,5-Dimethoxy-6-isopropyl-3-<<4-<(trimethylsilyl)oxy>-3-cyclohexen-1-yl>methyl>-2,6-dihydro-1,4-pyrazine

Downstream raw materials:

(R)-4-((2S,5R)-5-Isopropyl-3,6-dimethoxy-2,5-dihydro-pyrazin-2-ylmethyl)-cyclohex-2-enol

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