(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

Base Information

Chemical Name:(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene
CAS No.:716361-87-4
Molecular Formula:C₄₃H₃₅NO₆
Molecular Weight:661.754
Hs Code.:

Synonyms:(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

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Chemical Property of (E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

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Technology Process of (E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

There total 11 articles about (E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 716361-86-3
(E)-1-[3'-(4''-t-butylbenzoyl)benzamido-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

: 716361-87-4
(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 1h;
DOI:10.1081/SCC-120030700

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 716361-87-4
(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / potassium carbonate / dimethylformamide / 18 h / 100 °C

2: 88 percent / LiAlH₄ / diethyl ether / 4 h / 20 °C

3: 42 percent / phosphorous tribromide / CH₂Cl₂ / 5 h / 0 - 20 °C

4: 92 percent / tetrabutylammonium iodide / 18 h / 110 - 130 °C

5: 50 percent / potassium t-butoxide / dimethylformamide / 4 h / 20 °C

6: 56 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CHCl₃ / 18 h / Heating

7: 90 percent / trifluoroacetic acid / 1 h / 0 °C

With lithium aluminium tetrahydride; potassium tert-butylate; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1081/SCC-120030700

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 716361-87-4
(E)-1-[3'-(4''-carboxybenzamido)-4'-benzyloxy]phenyl-2-(3''',5'''-dibenzyloxy)phenylethene

Guidance literature:: Multi-step reaction with 5 steps

1: 42 percent / phosphorous tribromide / CH₂Cl₂ / 5 h / 0 - 20 °C

2: 92 percent / tetrabutylammonium iodide / 18 h / 110 - 130 °C

3: 50 percent / potassium t-butoxide / dimethylformamide / 4 h / 20 °C

4: 56 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CHCl₃ / 18 h / Heating

5: 90 percent / trifluoroacetic acid / 1 h / 0 °C

With potassium tert-butylate; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1081/SCC-120030700