(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

Base Information

Chemical Name:(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid
CAS No.:100257-22-5
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

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Technology Process of (rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

There total 4 articles about (rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 75-25-2
Bromoform

: 939-97-9
4-tert-Butylbenzaldehyde

: 100257-22-5
(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

Guidance literature:: With lithium chloride; potassium hydroxide; In 1,4-dioxane; at 0 - 35 ℃; for 60h; Reagent/catalyst; Solvent;
DOI:10.1002/ejoc.201700161

Reference yield:

: 7099-90-3
2-(4-(tert-butyl)phenyl)-2-oxoacetic acid

: 100257-22-5
(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; sodium acetate; triphenylphosphine; In methanol; at 20 ℃; under 7500.75 Torr;
DOI:10.1002/adsc.201700846

Reference yield:

: 253185-03-4,253185-04-5
tert-butylbenzene

: 609-09-6
Diethyl ketomalonate

: 100257-22-5
(rac)-2-(4-(tert-butyl)phenyl)-2-hydroxyacetic acid

Guidance literature:: With tin(IV) chloride; Erwaermen des Reaktionsprodukts mit wss. Kalilauge und Erwaermen der mit wss. Salzsaeure angesaeuerten Reaktionsloesung;
DOI:10.1021/ja01272a008