C₁₅H₂₂O₃

Base Information

• Chemical Name: C₁₅H₂₂O₃
• CAS No.: 1264271-95-5
• Molecular Formula: C₁₅H₂₂O₃
• Molecular Weight: 250.338
• Mol file: 1264271-95-5.mol

Synonyms:C₁₅H₂₂O₃

Chemical Property of C₁₅H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₂O₃

There total 3 articles about C₁₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C13H20O (1264272-23-2) + methyl chloroformate (79-22-1) → C15H22O3 (1264271-95-5)

Guidance literature:

C₁₃H₂₀O; With n-butyllithium; at -78 ℃; for 1h;

methyl chloroformate; at -78 - 20 ℃; for 15h;

With sodium hydrogencarbonate; In water;

DOI:10.1021/ol102989q

Reference yield:

C13H18O2 (1264272-21-0) → C15H22O3 (1264271-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / -78 °C / Inert atmosphere

2.1: diethyl ether / -78 - 20 °C

2.2: -20 °C

3.1: n-butyllithium / 1 h / -78 °C

3.2: 15 h / -78 - 20 °C

With n-butyllithium; diisobutylaluminium hydride; In diethyl ether; hexane; dichloromethane;

DOI:10.1021/ol102989q

Reference yield:

C12H16O → C15H22O3 (1264271-95-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diethyl ether / -78 - 20 °C

1.2: -20 °C

2.1: n-butyllithium / 1 h / -78 °C

2.2: 15 h / -78 - 20 °C

With n-butyllithium; In diethyl ether;

DOI:10.1021/ol102989q

upstream raw materials:

C₁₃H₁₈O₂

C₁₃H₂₀O

methyl chloroformate