2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol

Base Information

• Chemical Name: 2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol
• CAS No.: 55936-43-1
• Molecular Formula: C₁₂H₇Cl₂N₃O₃
• Molecular Weight: 312.112
• European Community (EC) Number: 667-561-7
• DSSTox Substance ID: DTXSID401040184
• Nikkaji Number: J3.466.245B

Synonyms:55936-43-1;SCHEMBL16285336;DTXSID401040184;AKOS024334313;2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol;Phenol, 2,6-dichloro-4-[2-(4-nitrophenyl)diazenyl]-

Chemical Property of 2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 310.9864465
• Heavy Atom Count: 20
• Complexity: 357

Purity/Quality:

98%+ ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1N=NC2=CC(=C(C(=C2)Cl)O)Cl)[N+](=O)[O-]

Technology Process of 2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol

There total 2 articles about 2,6-dichloro-4-[(E)-(4-nitrophenyl)diazenyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-Dichlorophenol (87-65-0) + 4-nitro-aniline (100-01-6,104810-17-5) → 4-hydroxy-3,5-dichlorophenylazo-4'-nitrobenzene (55936-43-1)

Guidance literature:

4-nitro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

2,6-Dichlorophenol; With sodium hydroxide; In water; at 0 - 5 ℃;

DOI:10.1080/15421406.2014.990239

Reference yield:

→ 4-hydroxy-3,5-dichlorophenylazo-4'-nitrobenzene (55936-43-1)

Guidance literature:

2,6-Dichlorphenol, 4-Nitrobenzoldiazonium Lsg.;

Reference yield: 65.0%

4-hydroxy-3,5-dichlorophenylazo-4'-nitrobenzene (55936-43-1) + C6H8NO2S(1+)*Cl(1-) → C18H14Cl2N4O5S

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 ℃; for 1h;

upstream raw materials:

2,6-Dichlorophenol

4-nitro-aniline

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