[(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride

Base Information

Chemical Name:[(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride
CAS No.:952023-91-5
Molecular Formula:C₁₈H₂₈Cl₂N₂P₂Pd
Molecular Weight:511.707
Hs Code.:

Synonyms:[(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride

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Chemical Property of [(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride

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Technology Process of [(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride

There total 2 articles about [(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 1107608-80-9,866081-62-1,959705-18-1
2,3-bis[(S)-(1,1-dimethylethyl)methylphosphino]quinoxaline

: 952023-91-5
[(S,S)-2,3-bis(tert-butylmethylphosphino)quinoxaline]palladium(II)dichloride

Guidance literature:: In toluene; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja502280w

Reference yield: 44.4%

: (dimethyl sulfoxide)2PdCl₂

: 1107608-80-9,866081-62-1,959705-18-1
(R,R)-(-)-2,3-bis(tert-butylmethylphosphino)qinoxaline

: 952023-91-5
((R,R)-(-)-2,3-bis(tert-butylmethylphosphino)quinoxaline)dichloropalladium(II)

Guidance literature:: In dichloromethane; to soln. ligand in CH2Cl2 soln. Pd complex in CH2Cl2 was added and stirred at room temp. for 2 h; soln. was concd. in vacuo, hexane was added, ppt. was filtered and dried;
DOI:10.1021/om700755y