1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

Base Information

Chemical Name:1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole
CAS No.:129423-45-6
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

Synonyms:1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

Chemical Property:

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Technology Process of 1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

There total 3 articles about 1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 129423-38-7
6-[5-Methoxy-2-(4-methoxy-phenyl)-3-methyl-indol-1-yl]-hexanoic acid benzylamide

: 129423-45-6
1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

Guidance literature:: With boron tribromide; In dichloromethane; 1.) -60 deg C, 2.) reflux, 2 h;
DOI:10.1021/jm00171a045

Reference yield:

: 91444-18-7
5-methoxy-2-(4-methoxyphenyl)-3-methyl-1H-indole

: 129423-45-6
1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMA, 0 deg C, sonication, 20 min, 2.) DMF, RT, 2 h

2: 43 percent / BBr₃ / CH₂Cl₂ / 1.) -60 deg C, 2.) reflux, 2 h

With boron tribromide; sodium hydride; In dichloromethane;
DOI:10.1021/jm00171a045

Reference yield:

: 22809-44-5
N-benzyl-6-bromohexanamide

: 129423-45-6
1-<5-(benzylcarbamoyl)pentyl>-5-hydroxy-2-(4-hydroxyphenyl)-3-methylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMA, 0 deg C, sonication, 20 min, 2.) DMF, RT, 2 h

2: 43 percent / BBr₃ / CH₂Cl₂ / 1.) -60 deg C, 2.) reflux, 2 h

With boron tribromide; sodium hydride; In dichloromethane;
DOI:10.1021/jm00171a045